4,5-Dichloro-3H-1,2-dithiol-3-one → HCID 20244134, compound

Participants

Reaction Steps

The procedure followed is analogous to that described in Example 1, but 4,5-dichloro-1,2-dithiol-3-one (3.16 g) and 2,3,4,5-tetrahydro-1H-benz[d]azepine (2.5 g) are used as starting substances, and, after recrystallization from acetonitrile, 4-chloro-5-(2,3,4,5-tetrahydro-1H-benz[d]azepin-3-yl)-1,2-dithiol-3-one (2.3 g) is obtained in the form of an ochre powder of m.p. 141° C.

Provenance & Evidence