m-Chloroperbenzoic acid → HCID 13589729, compound

HRID 482966Notes

Reaction equation

HRID 482966 reaction equation
[Cl:1][C:2]1[C:7]2[CH2:8][CH:9]([CH3:11])[O:10][C:6]=2[C:5]([NH:12][NH:13][C:14]([N:16]([O:18][CH3:19])[CH3:17])=[O:15])=[CH:4][C:3]=1[CH3:20].C1C=C(Cl)C=C(C(OO)=O)C=1.CC1CC2C=CC=C(NNC(N(OC)C)=O)C=2O1>>[Cl:1][C:2]1[C:7]2[CH2:8][CH:9]([CH3:11])[O:10][C:6]=2[C:5]([N:12]=[N:13][C:14]([N:16]([O:18][CH3:19])[CH3:17])=[O:15])=[CH:4][C:3]=1[CH3:20]

Participants

4

Reactant 3

HCID 70297m-Chloroperbenzoic acidHCID 135358281-(2,3-Dihydro-2-methylbenzofuran-7-yl)-4-methoxy-4-methylsemicarbazideHCID 135897281-(4-Chloro-2,3-dihydro-2,5-dimethylbenzofuran-7-yl)-4-methoxy-4-methylsemicarbazide

Product 1

HCID 13589729HCID 13589729, compound

Procedure

2 was prepared, as a yellow solid, by treating 2E with MCPBA according to the procedure and conditions described in Example 1 for preparing 1 from 1E.

Workup

  1. custom2 was prepared, as a yellow solid

Sources & evidence

ORD record
ord-50335f4094e34eb7a0f2201a0fdbd0b5
Source dataset
uspto-grants-1986_03
Patent number
US04577011

Reaction notes

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