HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Methyl-5,6,7,8-tetrahydroquinoline → HCID 178501895, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Methyl-5,6,7,8-tetrahydroquinoline | HCID 120028 | — |
| Reactant | HCID 122715448 | HCID 122715448 | — |
| Reactant | Butyllithium | HCID 178418339 | — |
| Product | HCID 178501895 | HCID 178501895 | — |
Reaction Steps
The title compound was prepared in a similar manner to that described in Example 1 using 5,6,7,8-tetrahydro-3-methylquinoline (0.01 M), butyl lithium (0.01 M) and dimethoxymethylsilyl chloride (0.015 M). The sample was distilled twice using a kugelrohr apparatus to give the title compound (0.25 g) bp 110°-120° C./0.5 mm.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04577022 |
| Source dataset | uspto-grants-1986_03 |
| ORD ID | ord-9e1923bed15644aaae3549d03cc52259 |
| Source note | uspto-grants-1986_03 |