HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Ether → HCID 54302294, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | Beta-Nitrostyrene | HCID 7626 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Ethyl Thioglycolate | HCID 12185 | — |
| Product | HCID 54302294 | HCID 54302294 | — |
Reaction Steps
To a solution of beta-nitrostyrene (447 mg) in ether (10 ml) are added triethylamine (42 l) and ethyl thioglycolate (0.33 ml). After 30 minutes' stirring, the mixture is concentrated to give (1-phenyl-2-nitroethyl)thioacetic acid ethyl ester (718 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04578378 |
| Source dataset | uspto-grants-1986_03 |
| ORD ID | ord-c89227822d924da78b9cd102179ba460 |
| Source note | uspto-grants-1986_03 |