HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Bromide → HCID 20242593, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Bromide | HCID 260 | — |
| Reactant | HCID 20242624 | HCID 20242624 | — |
| Product | HCID 20242593 | HCID 20242593 | — |
Reaction Steps
A solution of 1-(4-chlorophenyl)-3-dimethylamino-6-methoxy-1,4-dihydroisoquinoline hydrochloride hydrate (1.5 g) in 48% aqueous hydrobromic acid (200 ml) was heated at 120° C. for 2.5 h. The solution was evaporated to dryness in in vacuo and recrystallised from ethanol-ether to give the title compound, (2.53 g),
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04578393 |
| Source dataset | uspto-grants-1986_03 |
| ORD ID | ord-f8322ba6d73f44f69a61309fc4bd258a |
| Source note | uspto-grants-1986_03 |