Hydrochloric Acid → HCID 20299615, compound

Participants

Reaction Steps

The procedure is as in Example 1, but starting from 8-acetylamino-8-acetylaminomethyl-tricyclo[5.2.1.0/2,6]decane (1.97 g), in the form of the exo racemate, in a 6N solution (50 cc) of hydrochloric acid in water for 24 hours under reflux. Taking up the residue from the evaporation in ethanol (20 cc) and diethyl ether (80 cc), 6-amino-8-aminomethyl-tricyclo[5.2.1.0/2,6]decane dihydrochloride (1.26 g), is obtained, as the exo racemate, in the form of white crystals which melt at 273°-5° C.

Provenance & Evidence