HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 108450-75-5
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Methanol | HCID 887 | — |
| Reactant | 4-Nitro-3-phenyl-L-alanine | HCID 13706 | — |
| Product | 108450-75-5 | HCID 53395976 | — |
Reaction Steps
A solution of p-nitro-L-phenylalanine (12.6 g) and c.HCl (7.5 g) in methanol (150 ml) was refluxed for 1.5 hours and the solvent then evaporated in vacuo. The residue was triturated with ether and recrystallised from SVM to give the desired product as a off-white solid, [α]25 +15.3° (c=0.55, MeOH).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05225431 |
| Source dataset | uspto-grants-1993_07 |
| ORD ID | ord-71a8162ecd834347b161bb44eb91ad7d |
| Source note | uspto-grants-1993_07 |