Hydrochloric Acid → HCID 19752585, compound

Participants

Reaction Steps

A mixture of the product from step (a) (2.2 g), 10% Pd/C (400 mg) and 2N aqu. HCl (4.3 ml) in ethanol/water (27.8 ml, 3:5 v/v) was hydrogenated at room temperature and atmospheric pressure for 24 hours (uptake ca 200 ml). The mixture was filtered through celite, the residue washed with hot water and the filtrate evaporated in vacuo to give the desired product as a white solid (2.1 g).

Provenance & Evidence