反应详情

The (7-methoxynaphth-1-yl)acetyl chloride obtained above is dissolved in 200 ml of anhydrous ether. After cooling the solution in an ice/salt bath, 200 ml of concentrated aqueous ammonia solution are added with agitation. The mixture is agitated for 30 minutes and the precipitate formed is spun down and recrystallized in ethanol.

1. temperatureAfter cooling the solution in an ice/salt bath
2. customthe precipitate formed
3. customrecrystallized in ethanol