HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → 2-(7-Methoxynaphthalen-1-yl)acetamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | 2-(7-Methoxynaphthalen-1-yl)acetyl chloride | HCID 19385766 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | 2-(7-Methoxynaphthalen-1-yl)acetamide | HCID 15149127 | — |
Reaction Steps
The (7-methoxynaphth-1-yl)acetyl chloride obtained above is dissolved in 200 ml of anhydrous ether. After cooling the solution in an ice/salt bath, 200 ml of concentrated aqueous ammonia solution are added with agitation. The mixture is agitated for 30 minutes and the precipitate formed is spun down and recrystallized in ethanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05225442 |
| Source dataset | uspto-grants-1993_07 |
| ORD ID | ord-164ba8c86b26412083727fb95a2d5568 |
| Source note | uspto-grants-1993_07 |