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HRID483417

反应详情

EQUATION

反应方程式

HRID 483417 的结构方程式

REACTANTS

反应物

2
结构：CC(C)c1ccc(NN)cc1.Cl
HCID2733248

4-Isopropylphenylhydrazine hydrochloride

C9H15ClN2

结构：COC(=O)C(C)(C)CC(=O)CSC(C)(C)C
HCID14980531

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)c1ccc2c(c1)c(SC(C)(C)C)c(CC(C)(C)C(=O)O)n2Cc1ccc(Cl)cc1
HCID3651377

MK 886

C27H34ClNO2S

PROCEDURE

实验过程

Following the procedure of Example 10, but using 1-(p-chlorobenzyl)-1[-(4-(i-propyl)phenyl]hydrazine hydrochloride and methyl 2,2-dimethyl-5-(t-butylthio)-4-oxopentanoate as starting materials and hydrolysis at reflux, the title compound was prepared, mp 189°-192°.

WORKUP

后处理

  1. custommaterials and hydrolysis
  2. temperatureat reflux