HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Hydroxide → HCID 15157668, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | HCID 15157721 | HCID 15157721 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 15157668 | HCID 15157668 | — |
Reaction Steps
200 mg of 3-(1-Acetyl-5-methoxy-2-methyl-3-indolyl)quinuclidine are stirred on a steam bath for 16 hours with 100 mg of KOH in 7 ml of water and 14 ml of ethanol. The mixture is then worked up as is customary. 3-(5-methoxy-2-methyl-3-indolyl)quinuclidine is obtained; hydrochloride, m.p. 231.7°-234.0°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05227386 |
| Source dataset | uspto-grants-1993_07 |
| ORD ID | ord-73f030f0a7434dd6bbc4516a39e4830f |
| Source note | uspto-grants-1993_07 |