HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 10746272, compound → HCID 10793779, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 10746272 | HCID 10746272 | — |
| Reactant | HCID 178418287 | HCID 178418287 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 10793779 | HCID 10793779 | — |
Reaction Steps
To a solution of alcohol (1.2 g) from Step 2 in CH2Cl2 (25 mL) was added molecular sieves powder (1 g, flame dried) and PCC (1 g). After 40 min, the reaction mixture was poured on a plug of SiO2 (wet with Et2O), and eluted with Et2O. The solvent was evaporated to give the title product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05227399 |
| Source dataset | uspto-grants-1993_07 |
| ORD ID | ord-28f89fcbbac84046a2b166e2940db2a6 |
| Source note | uspto-grants-1993_07 |