1,8-Diazabicyclo(5.4.0)undec-7-ene → HCID 22743229, compound

Participants

Reaction Steps

2-(3-Bromophenyl)propylamine (9.7 g, 45.3 mmol) was combined with isopropylsulfonyl chloride (6.1 mL, 54.4 mmol), and DBU (10.2 mL, 68 mmol) in a manner analogous to the procedure described in example 2 to provide the final title compound, [2-(3-bromophenyl)propyl][(methylethyl)sulfonyl]amine, (4.5 g, 31%) as a white crystalline solid. Electron spray M.S. 320 (M*−H).

Provenance & Evidence