HuagongsheHuagongshe Chemistry Print Report · For research reference only
n-[2-(1-Methyl-5-{2-[(phenylmethoxy)carbonylamino]ethyl}benzimidazol-2-yl)ethyl](phenylmethoxy)carboxamide → HCID 12991239, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | n-[2-(1-Methyl-5-{2-[(phenylmethoxy)carbonylamino]ethyl}benzimidazol-2-yl)ethyl](phenylmethoxy)carboxamide | HCID 12991238 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | HCID 12991239 | HCID 12991239 | 55% |
Reaction Steps
N-[2-(1-Methyl-5-{2-[(phenylmethoxy)carbonylamino]ethyl}benzimidazol-2-yl)ethyl](phenylmethoxy)carboxamide (3.6 mmol) and 10% palladium on carbon (1.0 g, 62 mole %) were combined and hydrogenation was carried out in a manner analogous to the procedure described in example 6 to provide the intermediate title compound, 2-[5-(2-aminoethyl)-1-methylbenzimidazol-2-yl]ethylamine, (55%) as a colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06703425B2 |
| Source dataset | uspto-grants-2004_03 |
| ORD ID | ord-4dcd7b15a71b4485ad8cfeb7d00dfc15 |
| Source note | uspto-grants-2004_03 |