HRID48408

反应详情

EQUATION

反应方程式

HRID 48408 的结构方程式

PROCEDURE

实验过程

Using 2-chloro-1-thia-2,3,5,7-tetraazaindene (50 mg, 0.29 mmol) (see J. Org. Chem. 26, 4961 (1961), J. Chem. Soc. (C) 1856 (1967)) and 2-aminoindan (120 mg, 0.90 mmol), a similar procedure to Production Example 190 was carried out. The product obtained was purified by silica gel chromatography (hexane:ethyl acetate=3:1) to obtain the title compound (41 mg, 0.15 mmol) having the following physical properties:

WORKUP

后处理

  1. customThe product obtained
  2. customwas purified by silica gel chromatography (hexane:ethyl acetate=3:1)