HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromopropane → HCID 19750837, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromopropane | HCID 6358 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | HCID 10131121 | HCID 10131121 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 19750837 | HCID 19750837 | — |
Reaction Steps
A mixture of 2.5 g of 6-(methylsulfonyl)-benz[cd]indol-2(1H)-one (Example 3), 0.6 g of sodium hydride and 2.7 ml of 2-bromopropane in 100 ml of N,N-dimethylformamide is reacted for 18 hours under argon using the conditions of Example 4 to yield 2.24 g of the desired product as a yellow solid, m.p. 164°-165° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05229411 |
| Source dataset | uspto-grants-1993_07 |
| ORD ID | ord-6aac75ab899b43d9bbceebc9da54ea2f |
| Source note | uspto-grants-1993_07 |