HuagongsheHuagongshe Chemistry Print Report · For research reference only
Butyl iodide → HCID 19750825, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Butyl iodide | HCID 10962 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | HCID 19750821 | HCID 19750821 | — |
| Product | HCID 19750825 | HCID 19750825 | — |
Reaction Steps
A mixture of 2.15 g of 6-(methylthio)-benz[cd]indol-2(1H)-one (Example 12), 0.6 g of 60% sodium hydride and 1.7 ml of butyl iodide in 70 ml are reacted as described in Example 16 giving 1.85 g of the desired product as a solid, m.p. 75°-77° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05229411 |
| Source dataset | uspto-grants-1993_07 |
| ORD ID | ord-4d7550a92b6d4073bc9b0cc39eb07d0a |
| Source note | uspto-grants-1993_07 |