Hydroxyamine hydrochloride → HCID 73658850, compound

HRID 484345Notes

Reaction equation

HRID 484345 reaction equation
[CH:1]1([C:6]([C:8]2[CH:13]=[CH:12][C:11]([O:14][CH2:15][C:16]3[CH:25]=[CH:24][C:23]4[C:18](=[CH:19][CH:20]=[CH:21][CH:22]=4)[N:17]=3)=[CH:10][CH:9]=2)=O)[CH2:5][CH2:4][CH2:3][CH2:2]1.Cl.[NH2:27][OH:28]>>[CH:1]1([C:6]([C:8]2[CH:13]=[CH:12][C:11]([O:14][CH2:15][C:16]3[CH:25]=[CH:24][C:23]4[C:18](=[CH:19][CH:20]=[CH:21][CH:22]=4)[N:17]=3)=[CH:10][CH:9]=2)=[N:27][OH:28])[CH2:5][CH2:4][CH2:3][CH2:2]1

Participants

3

Reactant 2

HCID 443297Hydroxyamine hydrochlorideHCID 20084222HCID 20084222, compound

Product 1

HCID 73658850HCID 73658850, compound

Procedure

In analogy to the procedure of Example IV, the title compound is prepared from 20 g (60.3 mmol) of the compound from Example VIII and 6.3 g (90.7 mmol) of hydroxylamine hydrochloride.

Sources & evidence

ORD record
ord-f3b95505308541d38a97b8a178b7c9cc
Source dataset
uspto-grants-1993_07
Patent number
US05231103

Reaction notes

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