HuagongsheHuagongshe Chemistry Print Report · For research reference only
4'-Hydroxyacetophenone → Ethyl 4-(5,5,8,8-tetramethyl-5,6,7,8-tetrahydro-2-naphthoyloxy)benzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4'-Hydroxyacetophenone | HCID 7469 | — |
| Reactant | HCID 19888663 | HCID 19888663 | — |
| Product | Ethyl 4-(5,5,8,8-tetramethyl-5,6,7,8-tetrahydro-2-naphthoyloxy)benzoate | HCID 19748015 | — |
Reaction Steps
4-Acetylphenyl 5,5,8,8-tetramethyl-5,6,7,8-tetrahydro-2-naphthoate-Using 4-acetylphenol, the title compound was synthesized as a white solid. PMR (CDCl3): δ 1.36 (6H, s), 1.38 (6H, s), 1.76 (4H, s), 2.64 (3H, s), 7.34 (2H, d, J~8.4 Hz), 7.48 (1H, d, J~8.4 Hz), 7.98 (1H, dd, J~8.4 Hz, 2.4 Hz), 8.07 (2H, d, J~8.4 Hz), 8.19 (1H, d, J~2.4 Hz).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05231113 |
| Source dataset | uspto-grants-1993_07 |
| ORD ID | ord-41abf808409541ccb263e3c6f2a8f1a4 |
| Source note | uspto-grants-1993_07 |