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Alanine-methacrylamide → HCID 178449942、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Alanine-methacrylamide | HCID 86759378 | — |
| 反応物 | HCID 178449946 | HCID 178449946 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | HCID 178449942 | HCID 178449942 | — |
反応手順
Arginine-methacrylamide hydrochloride(10.53 g) and 13.90 g of the aforementioned alanine-methacrylamide were dissolved in 100 ml of distilled water, and bubbled with nitrogen gas for 1 hour. Potassium persulfate(250 mg) was added to the solution, and dissolved in it. The reaction mixture was refluxed by heating for 3 hours, then cooled to room temperature, and poured into acetone, so that precipitates were deposited. The supernatant was discarded, and acetone was again added to the precipitates and obtained mixture was stirred. The deposition was collected by filtration and dried to obtain the target polymer (white powder, 20.90 g).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06703468B1 |
| 出典データセット | uspto-grants-2004_03 |
| ORD ID | ord-2dbb898dd13a4e53b69224bbf57f53a4 |
| 出典メモ | uspto-grants-2004_03 |