4-Nitrobenzaldehyde → HCID 54324657, compound

HRID 484670Notes

Reaction equation

HRID 484670 reaction equation
[CH3:1][C:2]1[C:11]([CH3:12])=[N:10][C:9]2[C:4](=[CH:5][CH:6]=[CH:7][CH:8]=2)[N:3]=1.[N+:13]([C:16]1[CH:23]=[CH:22][C:19]([CH:20]=O)=[CH:18][CH:17]=1)([O-:15])=[O:14]>C(OC(=O)C)(=O)C>[N+:13]([C:16]1[CH:23]=[CH:22][C:19]([CH:20]=[CH:12][C:11]2[C:2]([CH:1]=[CH:20][C:19]3[CH:22]=[CH:23][C:16]([N+:13]([O-:15])=[O:14])=[CH:17][CH:18]=3)=[N:3][C:4]3[C:9](=[CH:8][CH:7]=[CH:6][CH:5]=3)[N:10]=2)=[CH:18][CH:17]=1)([O-:15])=[O:14]

Participants

4

Reactant 2

HCID 5414-NitrobenzaldehydeHCID 169252,3-Dimethylquinoxaline

Product 1

HCID 54324657HCID 54324657, compound

Reagents, catalysts & solvents 1

HCID 7918Acetic AnhydrideSolvent

Procedure

In 200 ml of acetic anhydride, 16 g of 2,3-dimethylquinoxaline and 30 g of p-nitrobenzaldehyde were heated under reflux for 30 minutes.

Workup

  1. temperatureunder reflux for 30 minutes

Sources & evidence

ORD record
ord-5c7ae97daabc4c44b8a1684756a25277
Source dataset
uspto-grants-1985_08
Patent number
US04533613

Reaction notes

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