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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 484699Generated: October 30, 2026

p-Toluenesulfonic acid → HCID 20272013, compound

https://huagongshe.com/reaction/484699

Reaction equation

Participants

RoleNameHCIDCharge
Reactantp-Toluenesulfonic acidHCID 6101—
ReactantHCID 20272009HCID 20272009—
SolventDiethyl EtherHCID 3283—
ProductHCID 20272013HCID 20272013—

Reaction Steps

A solution of 0.49 g. of p-toluenesulfonic acid in 50 ml. of diethyl ether was added to a solution of 1.00 g. of 6-(4-fluorophenyl)-2,3-bis(4-methoxyphenyl)pyridine in 50 ml. of diethyl ether. The resulting light yellow precipitate was recovered by filtration affording 1.29 g. of the desired title product, m.p. about 166°-167° C.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04533666
Source datasetuspto-grants-1985_08
ORD IDord-949c480f9bd44237bad25e2476d158a6
Source noteuspto-grants-1985_08