Methanol → HCID 70466056, compound

Participants

Reaction Steps

The title compound was prepared by the method of Example 26 using the product compound of Example 9 and excess methanol. The crude product was dissolved in the minimum amount of methanol and treated with diethyl ether to point of cloudiness, then cooled. Insolubles were removed by filtration and the product forced out of the filtrate by addition of ether, giving the title compound as a solid. Structure assignment was supported by the nmr spectrum and by elemental analysis.

Provenance & Evidence