Hydrochloric Acid → HCID 13048313, compound

Participants

Reaction Steps

To an ice-cooled solution of L-phenylalanine (16.5 g., 0.1 m) in 1N NaOH (100 ml) to which solid Na2CO3 (5.3 g, 0.05 m) had been added was added to the methyl chloroformate (7.8 ml, 0.1 m). Stirring was continued for 1/2 hr. with cooling and 1/2 hr. without. The mixture was carefully acidified with concentrated HCl to pH 2-3. After extraction with CH2Cl2 and drying (Na2SO4), evaporation of the solvent left

Provenance & Evidence