HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 1-(3-Diethylaminopropyl)-3-amino-4-chloroindazole dihydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | 1-(3-Diethylaminopropyl)-3-amino-4-chloroindazole | HCID 13229325 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 1-(3-Diethylaminopropyl)-3-amino-4-chloroindazole dihydrochloride | HCID 20135905 | — |
Reaction Steps
In 15 ml of absolute ethyl alcohol was dissolved 1.50 g of 1-(3-diethylaminopropyl)-3-amino-4-chloroindazole and into the solution was introduced dried hydrogen chloride gas under cooling with ice. To the solution was added anhydrous diethyl ether to separate crystals. Then the crystals were obtained by filtration and dried to give 1-(3-diethylaminopropyl)-3-amino-4-chloroindazole dihydrochloride having the following analytical value.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04533731 |
| Source dataset | uspto-grants-1985_08 |
| ORD ID | ord-b3b956e2409643ceb8689a79a9e7c5ae |
| Source note | uspto-grants-1985_08 |