HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 1-(3-Diethylaminopropyl)-3,5-diaminoindazole trihydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | 1-[3-(Diethylamino)propyl]-1H-indazole-3,5-diamine | HCID 20135839 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 1-(3-Diethylaminopropyl)-3,5-diaminoindazole trihydrochloride | HCID 20135838 | — |
Reaction Steps
In 15 ml of absolute ethyl alcohol was dissolved 0.6 g of 1-(3-diethylaminopropyl)-3,5-diaminoindazole, and into the solution was introduced dried hydrogen chloride gas under cooling with ice. To the solution was added anhydrous diethyl ether to separate crystals. Then the crystals were obtained by filtration and dried to give 1-(3-diethylaminopropyl)-3,5-diaminoindazole trihydrochloride having the following analytical value.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04533731 |
| Source dataset | uspto-grants-1985_08 |
| ORD ID | ord-58b986704ff846cdbed53a10946384f6 |
| Source note | uspto-grants-1985_08 |