HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86740233, compound → HCID 86740231, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86740233 | HCID 86740233 | — |
| Solvent | Hydrogen chloride-ethyl acetate | HCID 21866389 | — |
| Product | HCID 86740231 | HCID 86740231 | 103.9% |
Reaction Steps
A solution of N2 -(tert-butyloxycarbonyl)-N2 -ethyl-N-(3-phenylpropyl)-D-alaninamide (4.28 g.) in hydrogen chloride-ethyl acetate (3.9N, 35 ml.) was stirred for twenty minutes at room temperature, then concentrated. The residue was stripped of volatiles under vacuum (0.1 mm.) at room temperature, affording N2 -ethyl-N-(3-phenylpropyl)-D-alaninamide (3.22 g.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04533655 |
| Source dataset | uspto-grants-1985_08 |
| ORD ID | ord-77259e775e1441749949fc81b90a16d8 |
| Source note | uspto-grants-1985_08 |