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HRID484933

反应详情

EQUATION

反应方程式

HRID 484933 的结构方程式

REACTANTS

反应物

1
结构：C[C@H](C(=O)NCCCc1ccc(F)cc1)N(C)C(=O)OC(C)(C)C.N#N
HCID86740236

未命名化合物

PRODUCTS

生成物

1
结构：CN[C@H](C)C(=O)NCCCc1ccc(F)cc1.N#N
HCID86740238

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCOC(C)=O.Cl
溶剂HCID21866389

未命名化合物

PROCEDURE

实验过程

A solution of N2 -(tert-butyloxycarbonyl)-N2 -methyl-N-[3-(4-fluorophenyl)propyl]-D-alaninamide (2.77 g.) in hydrogen chloride-ethyl acetate (3.4N, 15 ml.) was stirred for thirty minutes at room temperature, then concentrated, affording N2 -methyl-N-[3-(4-fluorophenyl)propyl]-D-alaninamide as a crystalline solid (2.06 g., m.r. 148°-150° C.).

WORKUP

后处理

  1. concentrationconcentrated