Dimethylcarbamoyl Chloride → HCID 13469315, compound

HRID 484998Notes

Reaction equation

HRID 484998 reaction equation
[OH:1][CH:2]1[CH:6]([OH:7])[S:5][C:4](=[C:8]([C:15]([O:17][CH2:18][CH2:19][CH3:20])=[O:16])[C:9]([O:11][CH2:12][CH2:13][CH3:14])=[O:10])[S:3]1.[CH3:21][N:22]([CH3:26])[C:23](Cl)=[O:24]>N1C=CC=CC=1>[CH3:21][N:22]([CH3:26])[C:23]([O:7][CH:6]1[CH:2]([O:1][C:23](=[O:24])[N:22]([CH3:26])[CH3:21])[S:3][C:4](=[C:8]([C:15]([O:17][CH2:18][CH2:19][CH3:20])=[O:16])[C:9]([O:11][CH2:12][CH2:13][CH3:14])=[O:10])[S:5]1)=[O:24]

Participants

4

Reactant 2

HCID 6598Dimethylcarbamoyl ChlorideHCID 13490322HCID 13490322, compound

Product 1

HCID 13469315HCID 13469315, compound

Reagents, catalysts & solvents 1

HCID 1049PyridineSolvent

Procedure

1.0 g (3.1 m mole) of di-n-propyl 4,5-dihydroxy-1,3-dithiolane-2-ylidenemalonate was dissolved in 5 ml of pyridine, 1.33 g of N,N-dimethylcarbamoyl chloride was dropped into the solution, which was stirred for 18 hours at room temperature.

Sources & evidence

ORD record
ord-316ebbe120224a428a10dbf64af68401
Source dataset
uspto-grants-1985_08
Patent number
US04535075

Reaction notes

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