HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl chloride → N-(3-Methyl-2-oxobutyl)benzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl chloride | HCID 7412 | — |
| Reactant | Sodium Bicarbonate | HCID 516892 | — |
| Reactant | 1-Amino-3-methylbutan-2-one hydrochloride | HCID 13401736 | — |
| Product | N-(3-Methyl-2-oxobutyl)benzamide | HCID 13490305 | 90.5% |
Reaction Steps
4.5 g of isobutyrylmethylamine hydrochloride, 11 g of sodium bicarbonate and 4.81 g of benzoyl chloride are treated in the same manner as described in Preparation 1-(4). 6.07 g of N-benzoylisobutyrylmethylamine are thereby obtained. Yield: 90.5%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04535089 |
| Source dataset | uspto-grants-1985_08 |
| ORD ID | ord-46595f3b9bd7476498cdb89e27b7c56d |
| Source note | uspto-grants-1985_08 |