HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chlorobenzoyl chloride → 4-Chloro-N-(4-methyl-2-oxopentyl)benzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chlorobenzoyl chloride | HCID 8501 | — |
| Reactant | Sodium Bicarbonate | HCID 516892 | — |
| Reactant | 1-Amino-4-methylpentan-2-one hydrochloride | HCID 13701755 | — |
| Product | 4-Chloro-N-(4-methyl-2-oxopentyl)benzamide | HCID 13490307 | 97.5% |
Reaction Steps
3.8 g of isovalerylmethylamine hydrochloride, 5.04 g of sodium bicarbonate and 4.9 g of 4-chlorobenzoyl chloride are treated in the same manner as described in Preparation 1-(4). 6.2 g of N-(4-chlorobenzoyl)isovalerylmethylamine are thereby obtained. Yield: 98.0.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04535089 |
| Source dataset | uspto-grants-1985_08 |
| ORD ID | ord-7ca0d74dc2174541b0f38c4a8420904b |
| Source note | uspto-grants-1985_08 |