huagongshe.com
HRID485023

反应详情

EQUATION

反应方程式

HRID 485023 的结构方程式

REACTANTS

反应物

3
结构：O=C(Cl)c1ccc(Cl)cc1
HCID8501

4-Chlorobenzoyl chloride

C7H4Cl2O

结构：O=C([O-])O.[Na+]
HCID516892

Sodium Bicarbonate

CHNaO3

结构：CC(C)CC(=O)CN.Cl
HCID13701755

1-Amino-4-methylpentan-2-one--hydrogen chloride (1/1)

C6H14ClNO

PRODUCTS

生成物

1
结构：CC(C)CC(=O)CNC(=O)c1ccc(Cl)cc1
HCID13490307

4-Chloro-N-(4-methyl-2-oxopentyl)benzamide

C13H16ClNO2

收率 97.5%

PROCEDURE

实验过程

3.8 g of isovalerylmethylamine hydrochloride, 5.04 g of sodium bicarbonate and 4.9 g of 4-chlorobenzoyl chloride are treated in the same manner as described in Preparation 1-(4). 6.2 g of N-(4-chlorobenzoyl)isovalerylmethylamine are thereby obtained. Yield: 98.0.

WORKUP

后处理

  1. customas described in Preparation 1-(4)