Azobisisobutyronitrile → HCID 86740248, compound

HRID 485080Notes

Reaction equation

HRID 485080 reaction equation
[C:1]([O:4][CH:5]=[CH2:6])(=[O:3])[CH3:2].[CH3:7][O:8][C:9](=[O:17])[C:10]([S:12]([O:15][CH3:16])(=[O:14])=[O:13])=[CH2:11].N(C(C)(C)C#N)=NC(C)(C)C#N>>[C:1]([O:4][CH:5]=[CH2:6])(=[O:3])[CH3:2].[CH3:7][O:8][C:9](=[O:17])[C:10]([S:12]([O:15][CH3:16])(=[O:14])=[O:13])=[CH2:11]

Participants

4

Reactant 3

HCID 6547AzobisisobutyronitrileHCID 7904Vinyl AcetateHCID 54531152Methyl 2-(methoxysulfonyl)prop-2-enoate

Product 1

HCID 86740248HCID 86740248, compound

Procedure

After tempering at 65° C. and an increase in the viscosity of the mixture, a solution of 80 g of vinyl acetate, 20 g of 2-methoxysulphonyl propenoic acid methyl ester (11 mole percent) and 0.4 g of 2,2'-azo-bis-isobutyronitrile was added over a period of 1 hour.

Workup

  1. customAfter tempering at 65° C.
  2. temperaturean increase in the viscosity of the mixture

Sources & evidence

ORD record
ord-33a655bbce40473ca6fd5d3f56c1bd23
Source dataset
uspto-grants-1985_08
Patent number
US04535139

Reaction notes

Loading…