HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Iodide → HCID 13092097, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Iodide | HCID 5238 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Ethyl 4-(bromomethyl)benzoate | HCID 954261 | — |
| Reactant | HCID 20271536 | HCID 20271536 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 13092097 | HCID 13092097 | — |
Reaction Steps
2-Acetylamino-6-hydroxybenzaldehyde (0.45 g, 0.0025 M), ethyl 4-bromomethylbenzoate (0.51 g, 0.0025 M), anhydrous potassium carbonate (0.38 g), sodium iodide (50 mg) and 95% ethanol (20 ml) were reacted together (41/2 hr) to give ethyl 4-(3-acetylamino-2-formylphenoxymethyl)benzoate, m.p. 116°-119° C. (ethanol). (Found: C, 66.76; H, 5.61; N, 3.87%. C19H19NO5 requires C, 66,85; H, 5.61; N, 4.10%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04535183 |
| Source dataset | uspto-grants-1985_08 |
| ORD ID | ord-c5d0d353ee1b4f158b356e6b71272c56 |
| Source note | uspto-grants-1985_08 |