HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 20270153, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Sodium Methoxide | HCID 10942334 | — |
| Reactant | HCID 20270163 | HCID 20270163 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 20270153 | HCID 20270153 | — |
Reaction Steps
A solution of 4-(1-naphthyloxy)-butyl chloride (3.0 g) and sodium methoxide (1.5 g) in methanol (25 ml) was refluxed for 8 hours, then poured into water and the solution extracted with ether. The extract was dried and evaporated and the residue chromatographed on silica gel, eluting with 2:1 hexane ether, to produce the title compound as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04536503 |
| Source dataset | uspto-grants-1985_08 |
| ORD ID | ord-8541c8ad32bb4f06a2ebc031d588f634 |
| Source note | uspto-grants-1985_08 |