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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 485302Generated: October 29, 2026

Water → HCID 20270153, compound

https://huagongshe.com/reaction/485302

Reaction equation

Participants

RoleNameHCIDCharge
ReactantWaterHCID 962—
ReactantSodium MethoxideHCID 10942334—
ReactantHCID 20270163HCID 20270163—
SolventMethanolHCID 887—
ProductHCID 20270153HCID 20270153—

Reaction Steps

A solution of 4-(1-naphthyloxy)-butyl chloride (3.0 g) and sodium methoxide (1.5 g) in methanol (25 ml) was refluxed for 8 hours, then poured into water and the solution extracted with ether. The extract was dried and evaporated and the residue chromatographed on silica gel, eluting with 2:1 hexane ether, to produce the title compound as an oil.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04536503
Source datasetuspto-grants-1985_08
ORD IDord-8541c8ad32bb4f06a2ebc031d588f634
Source noteuspto-grants-1985_08