HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 20270154, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | HCID 13520555 | HCID 13520555 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 20270154 | HCID 20270154 | — |
Reaction Steps
A twofold stoichiometric excess of 3% hydrogen chloride in methanol is added to a solution of 1.0 g. of 1-(1-naphthyloxy)-8-(N,N-dimethylamino)octane in 20 ml methanol. Diethyl ether is added until precipitation is complete. The product is filtered, washed with ether, air dried and recrystallized to give 1-(1-naphthyloxy)-8-(N,N-dimethylamino)octane hydrochloride, m.p. 142°-143.5° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04536503 |
| Source dataset | uspto-grants-1985_08 |
| ORD ID | ord-a518a9935aca4316a92a60e687f8a4ba |
| Source note | uspto-grants-1985_08 |