Acetic Acid → HCID 53864591, compound

Participants

Reaction Steps

A solution of 1-methyl-5-[[4-[3-(1-piperidinylmethyl)phenoxy]butyl]amino]-1H-1,2,4-triazole-3-methanol (100 mg) in glacial acetic acid (5 ml) was heated under reflux for 8 h. The mixture was evaporated and the residue was triturated with ether to give the title compound as a white solid (97 mg) m.p. 119°-20°. tlc. System B,Rf 0.8.

Provenance & Evidence