HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(4-Hydroxyphenyl)-2-phenylbutan-1-one → 1-(4-Methoxyphenyl)-2-phenylbutan-1-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(4-Hydroxyphenyl)-2-phenylbutan-1-one | HCID 227278 | — |
| Reactant | 4-(beta-Dimethylaminoethoxy)-alpha-methyldesoxybenzoin | HCID 70479849 | — |
| Product | 1-(4-Methoxyphenyl)-2-phenylbutan-1-one | HCID 3642181 | — |
Reaction Steps
4-(β-Dimethylaminoethoxy)-α-ethyldesoxybenzoin (b.p. 162° C./0.075 mm.) may be obtained from α-ethyl-4-hydroxydesoxybenzoin by an analogous procedure to that described below for the preparation of 4-(β-dimethylaminoethoxy)-α-methyldesoxybenzoin, and α-ethyl-4-hydroxydesoxybenzoin itself (m.p. 122°-124° C.) may be obtained from α-ethyl-4-methoxydesoxybenzoin by an analogous procedure to that described below for the preparation of 4-hydroxy-α-methyldesoxybenzoin.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04536516 |
| Source dataset | uspto-grants-1985_08 |
| ORD ID | ord-74f512026c40454b863dc61d6094d425 |
| Source note | uspto-grants-1985_08 |