HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Hydroxide → HCID 13151846, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | 2-Chloro-5-nitrobenzoic acid | HCID 17287 | — |
| Reactant | m-Bromobenzenethiol | HCID 80597 | — |
| Catalyst | Copper | HCID 23978 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 13151846 | HCID 13151846 | — |
Reaction Steps
A mixture of 205 g. 3-bromothiophenol, 188 g. potassium hydroxide in 2 l. water, 205 g. 2-chloro-5-nitrobenzoic acid and 6.5 g. copper powder is refluxed for two hours, filtered while hot, acidified with hydrochloric acid and the solid filtered, washed with water and dried to yield 301 g. of the desired white solid, m.p. 202°-206° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04536507 |
| Source dataset | uspto-grants-1985_08 |
| ORD ID | ord-a1218ce042344b9fabf2d62df958b0af |
| Source note | uspto-grants-1985_08 |