HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 20270263, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | HCID 20270221 | HCID 20270221 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 20270263 | HCID 20270263 | — |
Reaction Steps
Reflux 200 mg. of 8-acetamido-10,11-dihydrodibenzo[b,f]thiepin-3-carboxylic acid for 16 hours in a mixture of 5 cc. of acetic acid and 5 cc. of 50% aqueous sulfuric acid. Dilute with water and separate the solids by filtration. Wash with water and dry to obtain the title product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04536507 |
| Source dataset | uspto-grants-1985_08 |
| ORD ID | ord-d4a694bf191440d0b5560e8f48a7673f |
| Source note | uspto-grants-1985_08 |