HuagongsheHuagongshe Chemistry Print Report · For research reference only
m-Chloroperbenzoic acid → 3-Cyano-8-hydroxydibenzo[b,f]thiepin-5-Oxide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | m-Chloroperbenzoic acid | HCID 70297 | — |
| Reactant | 3-Cyano-8-hydroxydibenzo[b,f]thiepine | HCID 13490384 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 3-Cyano-8-hydroxydibenzo[b,f]thiepin-5-Oxide | HCID 13490385 | — |
Reaction Steps
Suspend 50.2 mg. of 3-cyano-8-hydroxydibenzo[b,f]thiepine in 9 ml. of methylene chloride and add 40.6 mg. of m-chloroperbenzoic acid. Allow the mixture to stand at room temperature for 30 minutes. Separate the solids by filtration to obtain the title product (m.p., 241°-243° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04536507 |
| Source dataset | uspto-grants-1985_08 |
| ORD ID | ord-99ea53ce3589461f83a786116bfe841d |
| Source note | uspto-grants-1985_08 |