HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → o-Hydroxyphenyl methylcarbamate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | HCID 13269093 | HCID 13269093 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | o-Hydroxyphenyl methylcarbamate | HCID 82537 | — |
Reaction Steps
155 g of gaseous methylamine were fed into a solution of 680 g of pyrocatechol carbonate and 555 g of triethylamine in 2.5 liters of methylene chloride at 5° C., with vigorous stirring. 500 g of 36% strength hydrochloric acid were then added and the product was filtered off with suction and washed with water. 801 g (96% of the expected amount) of pyrocatechol methylcarbamate of melting point 125° C. were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04537986 |
| Source dataset | uspto-grants-1985_08 |
| ORD ID | ord-001923fd696c4864bc38ec8d342ec084 |
| Source note | uspto-grants-1985_08 |