HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 18599125, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | Hydroxyamine hydrochloride | HCID 443297 | — |
| Reactant | HCID 11116124 | HCID 11116124 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 18599125 | HCID 18599125 | — |
Reaction Steps
To a mixed solution of 8-oxo-cis-bicyclo[4,3,0]nona-3-ene (10 g), ethyl alcohol (100 ml), water (20 ml) and hydroxyamine hydrochloride (20 g), was added sodium hydroxide (37 g) at room temperature. After being stirred for one hour, the reaction mixture was poured into water. The crystals were gathered by filtration and washed with water. After drying, there was obtained 8-hydroxyimino-cis-bicyclo[4,3,0]nona-3-ene.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04537989 |
| Source dataset | uspto-grants-1985_08 |
| ORD ID | ord-01c0b9b9b3d841e88e2e798818fcfaf4 |
| Source note | uspto-grants-1985_08 |