HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 5-(2-Bromophenyl)-1H-tetrazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 5-(2-Bromophenyl)-1-(trimethylstannyl)-1H-tetrazole | HCID 20079345 | — |
| Solvent | Tetrahydrofuran toluene | HCID 22635083 | — |
| Product | 5-(2-Bromophenyl)-1H-tetrazole | HCID 178419373 | — |
Reaction Steps
To a solution of 1.0 g of 5-(2-bromophenyl)-1-(trimethylstannyl)-1H-tetrazole in toluene/THF (10:1) at room temperature is added HCl gas, via a bubbler. Gas addition is continued for 5 minutes after the appearance of a precipitate and the solid is then isolated by filtration and washed with hexanes.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05290780 |
| Source dataset | uspto-grants-1994_03 |
| ORD ID | ord-16d46d69f6254097b9ac3b233b300250 |
| Source note | uspto-grants-1994_03 |