反应详情

To a solution of 1.0 g of 5-(2-bromophenyl)-1-(trimethylstannyl)-1H-tetrazole in toluene/THF (10:1) at room temperature is added HCl gas, via a bubbler. Gas addition is continued for 5 minutes after the appearance of a precipitate and the solid is then isolated by filtration and washed with hexanes.

1. additionGas addition
2. customafter the appearance of a precipitate and the solid is then isolated by filtration
3. washwashed with hexanes