HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalic Acid → HCID 178520428, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalic Acid | HCID 971 | — |
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | HCID 178520427 | HCID 178520427 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 178520428 | HCID 178520428 | — |
Reaction Steps
0.5 (0.0017 mol) of 1-(3-phenylpropionyl)-4-(1H-imidazol-4-yl)piperidine and 1.2 equivalents of oxalic acid dissolved in 35 ml of isopropanol are brought to reflux for 1 h. After cooling, the precipitate obtained is drained,,washed with ethyl ether, dried and recrystallised in acetonitrile. A white powder is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05290790 |
| Source dataset | uspto-grants-1994_03 |
| ORD ID | ord-6e714b0aa8434d689d5abd929b323b13 |
| Source note | uspto-grants-1994_03 |