HuagongsheHuagongshe Chemistry Print Report · For research reference only
Butyl isocyanate → HCID 19097340, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Butyl isocyanate | HCID 8110 | — |
| Reactant | HCID 54389124 | HCID 54389124 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 19097340 | HCID 19097340 | — |
Reaction Steps
To a mixture of 1-(4-chlorobenzyl)-5-(aminoethoxy)-indole (1.0 g) in pyridine (I ml), butyl isocyanate (0.5 ml) was added at ambient temperature. After stirring for 15 minutes, excess pyridine was evaporated in vacuo and the residue recrystallized from ethanol to yield the title product, m.p. 163°-164° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05290788 |
| Source dataset | uspto-grants-1994_03 |
| ORD ID | ord-fb8cbba2fbac44c19ce842ae5c561366 |
| Source note | uspto-grants-1994_03 |