Diethyl Ether → HCID 131716731, compound

HRID 486097Notes

Reaction equation

[C:1]1([P:7](=[O:20])([C:14]2[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=2)[C:8]2[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[CH3:21][CH2:22][O:23][CH2:24][CH3:25]>>[C:1]1([P:7](=[O:20])([C:8]2[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=2)[C:14]2[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=2)[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=1.[CH3:21][CH2:22][O:23][CH2:24][CH3:25]

Participants

Reactant 2

HCID 3283Diethyl Ether

HCID 13097Triphenylphosphine Oxide

Product 1

HCID 131716731HCID 131716731, compound

Procedure

1H NMR indicated a product: triphenylphosphine oxide: ether molar ratio of 23:1:1.8 (mass % 93:4.7:2.2). Yield exclusive of triphenylphosphine oxide/ether, 40.06 g (72.5%).

Sources & evidence

ORD record: ord-97b8b4cd4f7c4ddd84614ab0421af86c
Source dataset: uspto-grants-1994_03
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05290799

Reaction notes

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