HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 178440893, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | HCID 178440892 | HCID 178440892 | — |
| Product | HCID 178440893 | HCID 178440893 | — |
Reaction Steps
The free base is obtained therefrom by adding aqueous ammonia solution, extracting the mixture with methyl tert-butyl ether, and drying and evaporating the organic phase to give a colorless oil (cis/trans mixture). Characteristic NMR data (CDCl3): cis-4-(4-tertbutylphenyl)cyclohexylamine: δ1-Heq =3.19; γ C-1=45.3 ppm.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05290806 |
| Source dataset | uspto-grants-1994_03 |
| ORD ID | ord-0072a8af84594b48b562174cdfd62079 |
| Source note | uspto-grants-1994_03 |